Analytical balance calibration is important if you want accurate readings of the materials being weighed every single time internal calibration. Us environmental protection agency office of pesticide programs. Us environmental protection agency office of pesticide. Calibration for analytical balances, industrial scales. The lab depot electronic balance calibration weights. Weighing scale calibration how to calibrate weighing.
Objective to lay down a procedure for operating and cleaning of analytical balance scope this sop shall provide the operating procedure of analytical balance of quality control department. Calibration is a very important to the accuracy of any balance. If the balance calibration is outofdate and requires a more thorough calibration than you can perform yourself, then. How to calibrate the electronic precision balance youtube. The standard operating procedure is applicable to in process quality assurance areas. Sop on procedure for operation of analytical balance. Check the balance leveling gauge to make sure bubble is inside the target. Medium accuracy calibrations of mass standards by modified substitution may 2019 job aids.
Operation, calibration and maintenance of electronic. We are precision weighing balances and you can order the epb10k from our web. Sop for calibration of balance standard operating procedure to evaluate the performance of analytical balance used for the analysis in pharmaceutical quality control by accuracy and precision tests. In order to weigh accurately with an electronic balance, the balance must be calibrated after it has been moved or if the room temperature has. Oppermann is out of print and the majority of content has been updated and. Nbs handbook 145, 1986, handbook for the quality assurance of metrological measurements, by john k. Standard operating procedures sops for balance testing. Weight scale calibration procedure memorial university. The measurement uncertainty of a balance, used for accurately weighing, must be determined.
Use a mild detergent, di water and lint free wipe if necessary. Make sure you have enough weights for the calibration procedure available. The original table of contents and several legacy sections are provided here as reference only. Calibration procedure for analytical balances and scales. Step by step instructions on how to select different calibration points and how to. Calibrated massesrequired for this procedure are to be such that the balance or scale may be loaded in iocrements equaltoonefourth,onehalf,three,fourths,and totalcapacity ofthebalanceorscale. If stringent calibration tolerances are required, this procedure should not be used. Before calibrating the balance, clean the weighing platforms. The good laboratory practices glps, good measurement practices gmps, and standard operating procedures sops that have not been updated are available on the linked pages as scanned pdf copies.
The balance is again in the weighing mode and ready for operation. If you purchase online, you will need to accomplish the calibration yourself, or bring in a scale dealer or. Unload the weight and repeat the procedure for all the weights. If the scale cannot be leveled or one of the feet is. At that time, he or she will calibrate the balance using a good class of certified weights. Electronically maintain an inventory of weigh balances. The lab depot how to calibrate balances and scales.
Weighing by single substitution using a single pan mechanical balance, a full electronic balance, or a balance with digital indications and built in weights may 2019 job aids. Applicable to all balances except analytical balances. To get all the accuracy your electronic balance andor scale provides, you need to perform routine calibrations and verifications using precision calibration weights. You will discover here a scale calibration procedure where most capabilities of a weighing scale will be checked for accuracy. The test load used in an eccentricity test should be at least one third of the max load of the weighing instrument.
Sop for operation and calibration of mettler toledo. The importance of balance calibration should not be underestimated, and it is crucial to weigh up the pros and cons of internal and external calibration before choosing your balance. Learn how to calibrate the sartorius ay412 electronic scale. Internal or external calibration for weighing scales.
Use tongs or gloves to place the empty container you will. A typical commercial calibration uses the manufacturers calibration procedure and is performed with a reference standard at least four times. Calibration for analytical balances, industrial scales, precision. Procedures will be consistent with sop adm07, nonconformance. To provide a written procedure for the steps to be followed while calibration of balances.
Refer to the balance operating manual to determine the calibration load. The weighing instrument should be switched on at least 30 minutes. Sop on calibration of weighing balance pharmastate blog. The following are guidelines for selecting the proper calibration weight for an electronic balance. The precision of the balance relies on minute factors and wind, shaky surfaces, or similar forces will cause the readings to be inaccurate. Recommendations on balance sensitivity, eccentricity and repeatability testing. Monthly calibration set the standard weights for various balances based on the capacity of the balance as mentioned in table i. Press the on button and wait for the balance to show zeroes on the digital screen. The calibration procedure should specify where to place the load during the test and calibration results in certificate format should also document the locations. A procedure performed to check a measuring instrument. To lay down a procedure for calibration of weighing balances.
Just as a musician must have one true tone to tune his instrument, a balance needs a true weight to tune itself. Quick calibration guide pdf 963kb products name language. Standards and equipment used must have a valid calibration certificate. It is recommended that this calibration be performed in an environment which is as. Hp, eki series with the user in mind making full digital calibration a cinch. If using an electronic balance, allow to warm up for at least 60 minutes. The larger denomination electronic balance calibration weights 5 kg and up have a recessed stainless steel grip handle for easy handling and stacking. This video is on the how to calibrate the epb10k digital scale. Measurement uncertainty must be reported in a calibration certificate, otherwise it is invalid. Hb 145 was developed as a source of calibration procedures for weights and measures laboratories and covered mass, length and volume calibrations for field standards used in the commercial marketplace. There is a bubblelevel just behind the digital readout.
It must be performed as per the manufacturers instructions. Balance calibration is the key service activity to ensure accurate weighing results. Standard operating procedure for the calibration of weight carts 33. Calibration of analytical balance answering the hows. Allow to stabilize for 15 to 20 seconds and then select the weight for calibration. In some laboratories, such as pharmaceutical labs, a balance will have its own specific calibration procedure and you need to follow this to abide by the necessary regulatory quality standards. I want to check the degree of drift in the balances sensitivity. It is because the reference standards for mass are weights, which are placed on a pan to inform the electronic balance that a given force is equivalent to a given number of grams, which is used for.
Place the electronic balance on a flat, stable surface indoors. Check the expiry date on the calibration sticker on the analytical balance if there is one. Electronic balances or scales use external calibration features that comparing the internal electronics to our class 1 standards. You will discover here a scale calibration procedure where most capabilities of a weighing scale will. The temperature at the balance is observed throughout the calibration process. Standard operating procedure to evaluate the performance of analytical balance used for the analysis in pharmaceutical quality control by accuracy and. Mechanical balance, a full electronic balance, or a balance with digital indications and built in weights 2015 added 2. This manual allows you to search for a function or operating procedure in a number of ways. Weighing scale calibration how to calibrate weighing instruments. Procedure and analysis calibration certificates must contain the stamp of the accrediting body e. Record the observations in the balance calibration record.